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Improvements in the hexachloroacetone/triphenylphosphine procedure for the conversion of allylic alcohols into chlorides

โœ Scribed by Magid, Ronald M.; Talley, Brenda G.; Souther, Stephen K.

Book ID
126242001
Publisher
American Chemical Society
Year
1981
Tongue
English
Weight
268 KB
Volume
46
Category
Article
ISSN
0022-3263

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๐Ÿ“œ SIMILAR VOLUMES

Hexachloroacetone/triphenylphosphine: A
Hexachloroacetone/triphenylphosphine: A reagent for the regio- and stereoselective conversion of allylic alcohols into chlorides
โœ Ronald M. Magid; O.Stanley Fruchey; William L. Johnson ๐Ÿ“‚ Article ๐Ÿ“… 1977 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 247 KB

The preparation of an allylic halide from the alcohol in a regio-and stereospecifically predictable fashion has been of concern to synthetic and mechanistic organic chemists. Numerous methods (of varying generality) have been developed, among which are the following: (a) reaction with conventional

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Temp. Time isolated Yields (%) Yields of (Equivs.) ("Cl (hrs) 2 2 2 or 11 I%) a None None lndole (1) lndole (2) lndole (3) lndole (3) Dihydropyran (3)