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Improvement of the purge- and -trap technique for the rapid analysis of volatile organic pollutants in water

✍ Scribed by Mehran, Mahrzad F. ;Nickelsen, M. G. ;Golkar, N. ;Cooper, W. J.


Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
414 KB
Volume
13
Category
Article
ISSN
0935-6304

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✦ Synopsis


Gas chromatography Megabore columns Rapid purge and trap Purgeable pollutants

As specified by the United States Environmental Protection Agency (USEPA) [5], P&T analysis involves an 11.0 rnin purge of a 5 mL sample at 40 mL/min followed by, a 4.0 min thermal listed in Table 2. The PID and ELCD were connected in series, with a 23 cm x 0.53 mm i.d. section of uncoated deactivated fused silica.


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## Abstract The potential of gas chromatography coupled to time‐of‐flight mass spectrometry (GC‐TOF MS) for the screening of organic pollutants in water was explored. After a conventional SPE step with C~18~ cartridges, the comparison of spectra with available libraries together with an evaluation