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Improved preparation of acetals of myo-inositol and its (±)-1-benzyl ether: conformational analysis of di-O-isopropylidene-myo-inositol derivatives

✍ Scribed by Roberto Fernandez de la Pradilla; Carlos Jaramillo; Jesus Jimenez-Barbero; Manuel Martin-Lomas; Soledad Penades; Amparo Zapata

Publisher
Elsevier Science
Year
1990
Tongue
English
Weight
664 KB
Volume
207
Category
Article
ISSN
0008-6215

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An improved procedure for the preparation of 1,2-O-isopropylidene-nqVo-inositol is described. Racemic 1,4-di-O-benzyl-2,3-O-isopropylidene-myo-inositol was prepared by tinmediated benzylation of 1,2-0-isopropylidene-myo-inositol and resolved readily by crystalk sation of the o-camphanates. The use o