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Improved preparation of 3-(1,1-dimethylallyl)decursinol

✍ Scribed by Xiangrui Jiang; Jianfeng Li; Rongxia Zhang; Hongli Guo; Shaolei Huang; Jingshan Shen

Publisher
Journal of Heterocyclic Chemistry
Year
2009
Tongue
English
Weight
63 KB
Volume
46
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

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An improved preparation method of 3‐(1,1‐dimethylallyl)decursinol from inexpensive commercially available start material was described. In the cyclization of 13, silica gel was used as catalyst to give 1 with high purity and satisfying yield. J. Heterocyclic Chem., 46, 560 (2009).

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