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Improved methods in the synthesis of 1α-hydroxylated vitamin D

✍ Scribed by Seok Si Toh; Tong Lan Ngiam; Lucy S.C. Wan; Sai Leung Leung

Book ID
116065618
Publisher
Elsevier Science
Year
1991
Tongue
English
Weight
358 KB
Volume
56
Category
Article
ISSN
0039-128X

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Crystal and molecular structure of 1α-hy
Crystal and molecular structure of 1α-hydroxylated analogs of vitamins D
✍ Waclaw Kolodziejski; Krzysztof Woźniak; Joanna Herold; Paulina M. Dominiak; Andr 📂 Article 📅 2005 🏛 Elsevier Science 🌐 English ⚖ 351 KB

Structures of two 1a-hydroxylated analogs of vitamins D, 1a-hydroxycholecalciferol and 1a-hydroxyergocalciferol, were solved and refined using single crystal X-ray diffraction. Crystallographic results are verified by 13 C CP/MAS NMR. This method provided also information on molecular mobility of an