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Improved methods for the radical deoxygenation of secondary alcohols

✍ Scribed by Derek H.R. Barton; Joseph Cs. Jaszberenyi

Book ID: 104229232
Publisher: Elsevier Science
Year: 1989
Tongue: French
Weight: 207 KB
Volume: 30
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)99080-4

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A~bsfrtsc~ seconbp] +whols wem hansfamed inte various thiaxrbonyl derivatives. Rcdaetiee of t&e eempuuads using t&&~hy$deandsnnmaloratTatiedthccomspoldingdeexy.eempetmds. Half-Rfeandeuapctitive meauaeme-etsshe~that mcttomwacfastaadcouldbenmtocomplctioh Deoxygenation of alcohols, especially secondar

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ChemInform Abstract: Phosphine-Boranes a

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Phosphine-Boranes as Selective Reagents for the Radical Deoxygenation of a Hindered Secondary Alcohol. -Refluxing the carbohydrate derived xanthates (I) and (III) with phosphine-borane in the presence of catalytic AIBN provides an efficient procedure for deoxygenation. -(BARTON,