Improved Method of Molecular Imprinting of Cyclodextrin on Silica-gel Surface for the Preparation of Stable Stationary HPLC Phase
β Scribed by TAKAHIKO MATSUI; TOMO OSAWA; KAZUMI SHIRASAKA; MAMI KATAYAMA; TAKAYUKI HISHIYA; HIROYUKI ASANUMA; MAKOTO KOMIYAMA
- Book ID
- 106388715
- Publisher
- Springer Netherlands
- Year
- 2006
- Tongue
- English
- Weight
- 357 KB
- Volume
- 56
- Category
- Article
- ISSN
- 0923-0750
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## Abstract In this study, the CD derivative, mono (6^A^βazidoβ6^A^βdeoxy)β__per__(__p__βchlorophenylcarbamonylated) Ξ²βCD was chemically immobilized onto the surface of an aminoβfunctionalized silica gel with different pore (100, 300, and 500Γ ) and particle (3, 5, and 10βΞΌm) sizes to obtain novel c
Immobilized chiral stationary phases (CSP)s from mono-6 A -azido-6 A -deoxy-perphenylcarbamoylated b-cyclodextrin were prepared using an extended application of the Staudinger reaction. Their application in preparative enantioseparations of racemic mixtures was demonstrated using atropine, bendroflu