## Abstract The increase in tissue sample temperature caused by the spinning of a rotor in high‐resolution magic‐angle spinning (HRMAS) NMR spectroscopy was investigated using two literature NMR thermometers. The classical methanol thermometer was used to calibrate the temperature difference betwee
✦ LIBER ✦
Improved analysis of tritiated samples via a 3H-NMR cryo-probe
✍ Scribed by Efstathios Alexakis; James P. Bloxsidge; John R. Jones; William J. S. Lockley
- Publisher
- John Wiley and Sons
- Year
- 2007
- Tongue
- French
- Weight
- 122 KB
- Volume
- 50
- Category
- Article
- ISSN
- 0022-2135
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✦ Synopsis
Abstract
Tritium (^3^H) NMR spectra of a number of compounds prepared via metal‐catalyzed H/T reduction/exchange of unsaturated hydrocarbons are presented. These show the considerable benefits that emerge from using a tritium cryo‐probe. Copyright © 2007 John Wiley & Sons, Ltd.
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