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Design and construction of a microcoil NMR probe for the routine analysis of 20-μL samples

✍ Scribed by Ian D. Henry; Gregory H.J. Park; Ravi Kc; Brian Tobias; Daniel Raftery


Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
307 KB
Volume
33B
Category
Article
ISSN
1552-5031

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A new probe design is presented for obtaining homonuclear, heteronuclear, and inverse detected NMR spectra from more than one sample in the same total data acquisition time as for a single sample, thus increasing data acquisition efficiency. Specifically, a two-coil system, with each solenoidal coil