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Identification of the Reaction Product of Δ8-Tetrahydrocannabinol with KN Reagent

✍ Scribed by D.T. Chia; S.A. Fike; J.T. Nelson

Book ID
104119081
Publisher
Elsevier
Year
1974
Tongue
English
Weight
406 KB
Volume
14
Category
Article
ISSN
0015-7368

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✦ Synopsis

As-Tetrahydrocannabinol reacts with tetrazotized o-dianisidine chloride to yield the ortho coupled dimer 2,2'-[(3,3'-dimethoxy-$,$I-biphenylene)bis(azo)] bis-As-tetrahydrocannabinol. JVMR and mass spectral data were used in the structure determination. Assignment of the aromatic proton resonances of the As-THC was made through the use of the lanthanide shift reagent, Eu(thd) , .

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Wittig-Horner reagents (1a-e) react with 1,3-dioxo-D 2,␣ -indanmalononitrile (2) to give the phosphonate adducts 3, 4, 5, 6, and 7, respectively. Structural reasoning for the new products was based on compatible analytical and spectral data (IR, 1 H, 31 P NMR, and MS). The mechanism that accounts fo