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Hypervalent iodine reagents: Synthesis of a steroidal orthoacetate by a radical reaction

✍ Scribed by Alicia Boto; Carmen Betancor; Ernesto Suárez

Book ID
103403383
Publisher
Elsevier Science
Year
1994
Tongue
French
Weight
313 KB
Volume
35
Category
Article
ISSN
0040-4039

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✍ Arun P Thottumkara; Thottumkara K Vinod 📂 Article 📅 2002 🏛 Elsevier Science 🌐 French ⚖ 126 KB

Allylic and benzylic alcohols are cleanly oxidized to the corresponding carbonyl compounds in water or water-THF mixtures using a water-soluble derivative of o-iodoxybenzoic acid. A mechanism involving single electron transfer steps is proposed for this facile and eco-friendly oxidation protocol.