Hydroxylation of phenol over Sn-silicalite-1 molecular sieve: solvent effects
β Scribed by Nawal Kishor Mal; Arumugamangalam V. Ramaswamy
- Publisher
- Elsevier Science
- Year
- 1996
- Tongue
- English
- Weight
- 1022 KB
- Volume
- 105
- Category
- Article
- ISSN
- 1381-1169
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π SIMILAR VOLUMES
Vanadium silicate molecular sieves with MEL structure (VS-2) are found to be active in the hydroxylation of phenol with hydrogen peroxide, a reaction which is commercially practiced over titanium silicalite (TS-1 and TS-2) catalysts. Among various reaction parameters, the influence of the solvent on
Titanium silicalite-1 samples of different particle size are synthesised and characterised by X-ray diffraction (XRD), photoelectron spectroscopy (XPS), diffuse reflectance spectroscopy (DRS), Raman and infrared spectroscopy. Size histograms are taken from transmission electron micrographs. Temporal