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Hydroxide-ion-initiated reactions under phase-transfer catalysis conditions. 9. Dehydrohalogenation of (haloethyl)benzenes by quaternary ammonium salts

✍ Scribed by Halpern, Marc; Zahalka, Hayder A.; Sasson, Yoel; Rabinovitz, Mordecai

Book ID: 126877053
Publisher: American Chemical Society
Year: 1985
Tongue: English
Weight: 648 KB
Volume: 50
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00225a019

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In addition, 14 (7 mg, 8%) was obtained. 4-tert-Butyl-l-hydroperoxy-9-oxabicyclo[4.2.l]nonanes (16 and 17). A solution of 14 (92 mg, 0.50 mmol) was rearrnged in THF (2 mL) and 90% H20z (2 mL, 72 mmol HzOz) containing TsOH.H,O (120 mg, 0.60 mmol) for 48 h according to procedure F. Preparative TLC of

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