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Hydrothermal Synthesis of Lindgrenite with a Hollow and Prickly Sphere-Like Architecture.

✍ Scribed by Jiasheng Xu; Dongfeng Xue


Publisher
John Wiley and Sons
Year
2007
Weight
13 KB
Volume
38
Category
Article
ISSN
0931-7597

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## Abstract Hollow sphere‐like carbides MC (M = Ti, V) with diameters of between 70 and 170 nm were synthesized via a template‐interface co‐reduction (TICR) route, in which MCl~4~ and hexachlorobuta‐1,3‐diene (C~4~Cl~6~) were reacted with metallic sodium at 500 °C for 24 h. X‐ray powder diffraction