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Hydrothermal Synthesis and Structural Characterization of a Novel Hydroxo Stannate: Sr2Sn(OH)8

✍ Scribed by Mingmei Wu; Xiuling Li; Guoping Shen; Jing Li; Ruren Xu; Davide M. Proserpio

Publisher
Elsevier Science
Year
2000
Tongue
English
Weight
237 KB
Volume
151
Category
Article
ISSN
0022-4596

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✦ Synopsis

A new hydroxo stannate(IV), Sr 2 Sn(OH) 8 , has been synthesized by the hydrothermal method. Single-crystal X-ray diffraction shows that this compound crystallizes in the monoclinic space group P 2 1 /c with a ‫؍‬ 6.006(1) A > , b ‫؍‬ 11.058(2) A > , c ‫؍‬ 6.129(2) A > , ‫؍‬ 112.98(2)3, V ‫؍‬ 374.8(2) A > 3 , Z ‫؍‬ 2, R ‫220.0؍‬ (I > 2 (I)). The structure [Sr(OH) 6/3 (OH) 2/2 ] 2 [Sn(OH) 6/3 ] consists of Sn(OH) 6 octahedra and Sr(OH) 8 triangulated dodecahedra. These Sr(OH) 8 and Sn(OH) 6 polyhedra form a novel complex 3D packing arrangement that contains channels running along [001], 5lled with the in-pointing hydrogens of the hydroxo groups.

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