An organic+inorganic hybrid solid, (Cu(2,2-bpy) 2 ) 2 Mo 8 O 26 , has been hydrothermally synthesized and structurally characterized by single-crystal X-ray di4raction. Dark green crystals crystallize in the orthorhombic system, space group Pna21, a ؍ 24.164(5), b ؍ 18.281(4), c ؍ 11.877(2) A
Hydrothermal Synthesis and Structural Characterization of a Novel Organic-Inorganic Hybrid Compound {[Cu (2, 2′-bpy)2]2-Mo8O26}
✍ Scribed by Yong-Hui Wang; Chen; Li-Dong; Chang-Wen Hu; Wang; En-Bo; Heng-Qing Jia; Ning-Hai Hu
- Publisher
- John Wiley and Sons
- Year
- 2010
- Tongue
- English
- Weight
- 518 KB
- Volume
- 20
- Category
- Article
- ISSN
- 0256-7660
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Two new compounds (TMA) 2 FeMo 6 O 20 and [TMA] 2 [Fe(H 2 O) 6 ]Mo 8 O 26 have been synthesized by hydrothermal reactions. (TMA) 2 FeMo 6 O 20 crystallizes in the monoclinic space group C2/m; a ؍ 21.204(1) A s s , b ؍ 7.6393(5) A s s , c ؍ 8.4191(6) A s s , ؍ 104.602(1)°°, V ؍ 1319.7(2) A