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Hydrothermal Synthesis and Crystal Structures of [(CH3NH3)0.5(NH4)1.5]Sb8S13·2.8H2O and Rb2Sb8S13 ·3.3H2O

✍ Scribed by Xiqu Wang; Lumei Liu; Allan J. Jacobson

Publisher: Elsevier Science
Year: 2000
Tongue: English
Weight: 437 KB
Volume: 155
Category: Article
ISSN: 0022-4596
DOI: 10.1006/jssc.2000.8942

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✦ Synopsis

The new thioantimonates [CH 3 NH 3 ) 0.5 (NH 4 ) 1.5 Sb 8 S 13 ' 2.8H 2 O (1) and Rb 2 Sb 8 S 13 ' 3.3H 2 O (2) have been hydrothermally synthesized and characterized by single-crystal structure determination. The two compounds are isostructural and crystallize in the monoclinic system, space group P2 1 /m with a ‫؍‬ 7.1931(3) A > ,

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