13C NMR characterization of acetonitrile
✍
J.A. Ripmeester; J.S. Tse; D.W. Davidson
📂
Article
📅
1982
🏛
Elsevier Science
🌐
English
⚖ 527 KB
Proton-decoupled 13C spectm ofC~~~-~qumol clathnte generally confirm Mfak and Lee's "drstorted" X-my stmcture. The smgle-eryst~ spectn gw shwidiag antsotroplcs of 13 and 293 ppm for the CH3 and CN groups, rcspectweiy. The CN triplet spbttmgs yrcld an mducct spur-spm coupling smsoiropy of ~430 Hz.