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Hydrogen-deuterium exchange reactions catalyzed by zerovalent phosphinepalladium complexes

✍ Scribed by Gordon K. Anderson; Antonia K. Phipps

Publisher
Elsevier Science
Year
1984
Tongue
English
Weight
295 KB
Volume
266
Category
Article
ISSN
0022-328X

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Preparation of deuterium-labeled rutin b
Preparation of deuterium-labeled rutin by hydrogen exchange reaction
✍ K. Hiraoka; T. Miyamoto; S. Baba; T. Furuta 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 258 KB

## Abstract Preparation of deuterium‐labeled rutin by hydrogen exchange reaction under alkaline condition is described. Hydrogens at positions 2′, 5′ and 6′ of rutin were replaced with deuteriums only on heating, while hydrogens at positions 6 and 8 were readily replaced at room temperature. On the