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Hybrid Open Frameworks. 8. Hydrothermal Synthesis, Crystal Structure, and Thermal Behavior of the First Three-Dimensional Titanium(IV) Diphosphonate with an Open Structure: Ti 3 O 2 (H 2 O) 2 (O 3 P−(CH 2 )−PO 3 ) 2 ·(H 2 O) 2 , or MIL-22

✍ Scribed by Serre, Christian; Férey, Gérard

Book ID
127201255
Publisher
American Chemical Society
Year
1999
Tongue
English
Weight
196 KB
Volume
38
Category
Article
ISSN
0020-1669

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Hydrothermal Synthesis, Powder Structura
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✍ M. Riou-Cavellec; C. Serre; J. Robino; M. Noguès; J.-M. Grenèche; G. Férey 📂 Article 📅 1999 🏛 Elsevier Science 🌐 English ⚖ 651 KB

Fe 2 (H 2 O) 2 (O 3 P+CH 2 +PO 3 H) 2 ](H 2 O) 2 or MIL-13 was prepared hydrothermally (120 h at 473 K). Its structure was determined by powder X-ray di4raction. This compound crystallizes in the triclinic system (P-1) with the following cell parameters: a ‫؍‬ 9.8487(6) A > , b ‫؍‬ 8.0308(5) A > , c

Hybrid Open Frameworks. Hydrothermal Syn
Hybrid Open Frameworks. Hydrothermal Synthesis, Structure Determinations, and Magnetic Behavior of (VIVO)2(H2O){O3P–(CH2)3–PO3}·2H2O: A New Vanado-alkyldiphosphonate Closely Related to VO(HPO4)·0.5H2O
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DEDICATED TO PROFESSOR J. M. HONIG (V IV O) 2 (H 2 O){O 3 P+(CH 2 ) 3 +PO 3 } ' 2H 2 O was hydrothermally synthesized from a mixture of VOSO 4 ' 5H 2 O : H 2 PO 3 + (CH 2 ) 3 +PO 3 H 2 : H 2 O in a molar ratio 1 : 0.5 : 250 and heated for 72 hours to 1703C. Its structure was determined from powder X