𝔖 Bobbio Scriptorium
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Homopolycondensation of di-(β-chloroethyl) phosphite and di-(β-chloroethyl) chlorophosphate

✍ Scribed by S.M. Shner; I.K. Rubtsova; Ye.L. Gefter


Book ID
118357242
Publisher
Elsevier Science
Year
1965
Weight
322 KB
Volume
7
Category
Article
ISSN
0032-3950

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is removed with concentrated hydrochloric acid. Distillation of the organic phase affords 13.1 g (14%) of ( 2), b.p. 31 OC/O.02 mm, yellow needles, m.p. 49 "C from methanol. It has A, , , = 295 mp, log E = 4.05 in cyclohexane, and infrared absorptions at 695 (m), 805 (s), 1000 (m), 1230 (s), and 149