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Highly Efficient Copper-Mediated Atom-Transfer Radical Addition (ATRA) in the Presence of Reducing Agent

✍ Scribed by William T. Eckenhoff; Sean T. Garrity; Tomislav Pintauer

Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
331 KB
Volume
2008
Category
Article
ISSN
1434-1948

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## Abstract One‐pot sequential reactions involving azide–alkyne [3+2] cycloaddition and atom transfer radical addition (ATRA) catalyzed by [Cu^II^(TPMA)X][X] {X = Br^–^ or Cl^–^, TPMA = tris(2‐pyridylmethyl)amine} in the presence of ascorbic acid as a reducing agent are reported. Reactions with azi