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Highly Efficient and Catalytic Conversion of Aldoximes to Nitriles

โœ Scribed by Yang, Soon Ha; Chang, Sukbok

Book ID
111885879
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
86 KB
Volume
3
Category
Article
ISSN
1523-7060

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Highly efficient Pd-catalyzed synthesis
Highly efficient Pd-catalyzed synthesis of nitriles from aldoximes
โœ Hoo Sook Kim; Sung Hwan Kim; Jae Nyoung Kim ๐Ÿ“‚ Article ๐Ÿ“… 2009 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 808 KB

An expedient method of Pd-catalyzed conversion of aldoxime into nitrile was developed. The reaction was carried out under the influence of Pd(OAc) 2 /PPh 3 in refluxing CH 3 CN to provide good to high yields. The use of Cs 2 CO 3 (0.1-0.5 equiv) was crucial in some cases.