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High-Yielding Preparation of a Stable Precursor of Hydroxytyrosol by Total Synthesis and from the Natural Glycoside Oleuropein

✍ Scribed by Gambacorta, Augusto; Tofani, Daniela; Bernini, Roberta; Migliorini, Antonella

Book ID
121317444
Publisher
American Chemical Society
Year
2007
Tongue
English
Weight
105 KB
Volume
55
Category
Article
ISSN
0021-8561

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## Abstract For Abstract see ChemInform Abstract in Full Text.

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Toward the total synthesis of pseudolaric acid B. Preparation of a key intermediate by degradation and its use in the reassembly of the natural product
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Synthetic studies of pseudolaric acid B, 2, provided a relay synthesis of pseudolaric acid B (PLAB) via aldehyde 5. The aldehyde 5 can serve: to complete the total synthesis of PLAB; as a precursor for the synthesis of PLAB analogs; or as a substrate for the generation of radiolabeled PLAB for mecha