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High sensitivity analysis of deuterium in solids by 15N-induced nuclear reactions

✍ Scribed by Shigeki Hayashi; Hisao Nagai; Michi Aratani; Tadashi Nozaki; Minoru Yanokura; Isao Kohno; Osamu Kuboi; Yoshifumi Yatsurugi

Book ID
113277512
Publisher
Elsevier Science
Year
1986
Tongue
English
Weight
500 KB
Volume
16
Category
Article
ISSN
0168-583X

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✍ Yoshitaka Ishii; Robert Tycko πŸ“‚ Article πŸ“… 2000 πŸ› Elsevier Science 🌐 English βš– 82 KB

Enhancement of sensitivity in solid state 15 N NMR by indirect detection through 1 H NMR signals under high-speed magic angle spinning and high-field conditions is demonstrated experimentally on two 15 N-labeled peptides, polycrystalline AlaGlyGly and the helix-forming, 17-residue peptide MB(i Ψ‰ 4)E