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High-resolution Tin-119 NMR of solid trimethyltin hydroxide

✍ Scribed by Robin K Harris; Kenneth J Packer; Patrick Reams


Publisher
Elsevier Science
Year
1985
Weight
152 KB
Volume
61
Category
Article
ISSN
0022-2364

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The ingh-resolution tin-1 19 NMR spectrum of sofrd tn(n-buiyl)tin fluoride s.h~ws t.hre equally spaced centrebands, in-&cating effectzvely equal CoupLtng of t lQSn to two ffuorine nuclei, which is consistent with pentacoordinated tin with a cham structure The spinntng sideband patterns illustrate th

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Tin-119, tin-117) coupling satellites are visible in the CP/MAR spectra of tetrakis(trimethylstanny1)methane and of a series of tetrastannacyclohexanes, the values in the solid and solution states being equal within experimental error. The single signal from the former compound has a line width of o