High Resolution NMR || The Use of NMR in Structure Elucidation

✍ Scribed by BECKER, EDWIN D.

• Book ID: 120927363
• Publisher: Elsevier
• Year: 1980
• Tongue: English
• Weight: 817 KB
• Edition: Subsequent
• Category: Article
• ISBN: 0120846608
• DOI: 10.1016/B978-0-12-084660-3.50011-2

✦ Synopsis

Origins And Early History Of Nmr -- High Resolution Nmr: An Overview -- The Theory Of Nmr -- Nuclear Spin And Magnetic Moment -- Theoretical Descriptions Of Nmr -- Steady-state Quantum Mechanical Description -- Effect Of The Boltzmann Distribution -- Spin-lattice Relaxation -- Precession Of Nuclear Magnetic Moments -- Classical Mechanical Description Of Nmr -- Magnetization In The Rotating Frame -- Methods Of Obtaining Nmr Spectra -- Dynamic Processes -- Terminology, Symbols, Units, And Conventions -- Instrumentation And Techniques -- Advantages Of Pulse Fourier Transform Nmr -- Basic Nmr Apparatus -- Requirements For High Resolution Nmr -- Detection Of Nmr Signals -- Phase Cycling -- Fourier Transformation Of The Fid -- Data Acquisition -- Data Processing -- Digital Filtering -- Alternatives To Fourier Transformation -- Sensitivity And Size Of Sample -- Useful Solvents -- Chemical Shifts -- The Origin Of Chemical Shifts -- Theory Of Chemical Shifts -- Measurement Of Chemical Shifts -- Empirical Correlations Of Chemical Shifts -- Some Aspects Of Proton Chemical Shifts -- Nuclei Other Than Hydrogen -- Compilations Of Spectral Data And Empirical Estimates Of Chemical Shifts -- Isotope Effects -- Effects Of Molecular Asymmetry -- Paramagnetic Species -- Coupling Between Pairs Of Spins -- Origin Of Spin Coupling Interactions -- General Aspects Of Spin-spin Coupling -- Theory Of Spin-spin Coupling -- Correlation Of Coupling Constants With Other Physical Properties -- Effect Of Exchange -- Spin Decoupling And Double Resonance. Edwin D. Becker. Includes Bibliographical References And Index.