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High resolution glass capillary columns for the gas chromatographic analysis of alditol acetates of neutral and amino sugars

✍ Scribed by Hudson, J. R. ;Morgan, S. L. ;Fox, A.

Publisher: John Wiley and Sons
Year: 1982
Tongue: English
Weight: 447 KB
Volume: 5
Category: Article
ISSN: 0935-6304
DOI: 10.1002/jhrc.1240050602

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✦ Synopsis

Abstract

The development of improved high resolulation glass capillary columns for separating the alditol acetates of neutral and amino sugars is described. Different capillary column treatments were evaluated for their activity toward amino sugar derivatives and for their effect on the efficiency of the completed column. The simple two‐step procedure of leaching with aqueous hydrochloric acid and dynamic coating with SP‐2330 was found to produce efficient and inert columns.

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