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High-pressure polymerization of phenylacetylene and of the benzene and acetylene moieties

✍ Scribed by Mario Santoro; Lucia Ciabini; Roberto Bini; Vincenzo Schettino

Publisher
John Wiley and Sons
Year
2003
Tongue
English
Weight
252 KB
Volume
34
Category
Article
ISSN
0377-0486

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Polymerization of phenylacetylene with W
Polymerization of phenylacetylene with WOCl4/tetraphenyltin catalyst in benzene/1,4-dioxane. Synthesis of high-molecular-weight poly(phenylacetylene)
✍ Jan Sedláček; Marta Pacovská; Jiří Vohlídal; Zlatka Grubišić-Gallot; Majda Žigon 📂 Article 📅 1995 🏛 John Wiley and Sons 🌐 English ⚖ 362 KB

Phenylacetylene was polymerized with WOCl,/tetraphenyltin (mole ratio 1 : 2) catalyst in benzene and benzene/ 1 ,4-dioxane mixtures. The resulting polymers were characterized by means of multidetector size-exclusion chromatography and ' H NMR and IR spectroscopy. 1,4-Dioxane used as a co-solvent was