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High-pressure high-temperature synthesis of Mn4Nb2O9. A XRD and TEM study

✍ Scribed by Alexander P. Tyutyunnik; Vladimir G. Zubkov; Tatjana V. D'yachkova; Yury G. Zainulin; Nadezhda V. Tarakina; Marı́a J. Sayagués; Gunnar Svensson


Book ID
114370617
Publisher
Elsevier Science
Year
2002
Tongue
English
Weight
663 KB
Volume
4
Category
Article
ISSN
1293-2558

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A new stannosilicate Cs 2 SnSi 3 O 9 has been synthesized and characterized by single-crystal X-ray diffraction and solid-state NMR spectroscopy. It crystallizes in the orthorhombic space group P2 1 2 1 2 1 (No. 19) with a ¼ 7:9612ð7Þ ( A; b ¼ 10:3444ð9Þ ( A; c ¼ 11:780ð1Þ ( A; V ¼ 970:1ð3Þ ( A 3 ;