High-performance liquid chromatography with fluorescence detection of ebiratide using 4-(N, N-dimethylamino-sulphonyl)-7-fluoro-2, 1, 3-benzoxadiazole as a fluorogenic reagent
โ Scribed by Yozo Hamachi; Tsuyosi Tsujiyama; Kenichiro Nakashima; Shuzo Akiyama
- Publisher
- John Wiley and Sons
- Year
- 1995
- Tongue
- English
- Weight
- 360 KB
- Volume
- 9
- Category
- Article
- ISSN
- 0269-3879
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A peroxyoxalate chemiluminescence detection in high-performance liquid chromatography was examined for determination of long chain aliphatic aldehydes using 4-(N~-dimethylaminosulphonyl)-7-hydrazino-2,~,3benzoxadiazole (DBD-H) as a fluorogenic labelling reagent. A mixture of 0.6 m M bi~(2,4,6-trichl
## Abstract Benzofurazan derivatization reagent, 4โ[2โ(__N__,__N__โdimethylamino)ethylaminosulfonyl]โ7โ__N__โmethylhydrazinoโ2,1,3โbenzoxadiazole (DAABDโMHz), for aldehydes in liquid chromatography/electrospray ionizationโtandem mass spectrometry (LC/ESIโMS/MS), was synthesized. DAABDโMHz reacted w