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High-Field Dynamic Nuclear Polarization for Solid and Solution Biological NMR

✍ Scribed by A. B. Barnes; G. De Paëpe; P. C. A. van der Wel; K.-N. Hu; C.-G. Joo; V. S. Bajaj; M. L. Mak-Jurkauskas; J. R. Sirigiri; J. Herzfeld; R. J. Temkin; R. G. Griffin

Book ID
106220493
Publisher
Springer Vienna
Year
2008
Tongue
English
Weight
698 KB
Volume
34
Category
Article
ISSN
0937-9347

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2H solid state NMR spectra of a polypeptide in an oriented membrane environment is demonstrated to have an orientational resolution of 0.3 degree. Such data results in high resolution structural constraints. Similar spectra are demonstrated at 23.2 T using a resistive magnet at the National High Mag