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Heterocyclic analogs of pleiadiene. 63. Synthesis and crystal structure of 1-aminoperimidines

✍ Scribed by A. F. Pozharskii; O. V. Kryshtalyuk; G. G. Aleksandrov; V. V. Kuz'menko

Publisher
Springer US
Year
1995
Tongue
English
Weight
659 KB
Volume
31
Category
Article
ISSN
0009-3122

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Structures of two 1a-hydroxylated analogs of vitamins D, 1a-hydroxycholecalciferol and 1a-hydroxyergocalciferol, were solved and refined using single crystal X-ray diffraction. Crystallographic results are verified by 13 C CP/MAS NMR. This method provided also information on molecular mobility of an