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Glycosidase−Substrate Interactions Analysis by STD-NMR Spectroscopy: Study of α- l -Fucosidase

✍ Scribed by Berteau, Olivier; Sandström, Corine; Bielicki, Julie; Anson, Donald S.; Kenne, Lennart

Book ID
120446239
Publisher
American Chemical Society
Year
2003
Tongue
English
Weight
52 KB
Volume
125
Category
Article
ISSN
0002-7863

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Structural analysis of methyl α-l-fucopyranoside by X-ray crystallography, NMR spectroscopy, and molecular mechanics calculations
✍ D. Lamba; A.L. Segre; G. Fabrizi; B. Matsuhiro 📂 Article 📅 1993 🏛 Elsevier Science 🌐 English ⚖ 422 KB

The crystal and molecular structures of methyl a-L-fucopyranoside are reported. The sugar ring has the expected 'C, conformation. The 'H NMR spectrum at 600 MHz was fully analysed. The conformation of the pyranose ring in solution, derived from 'JHH values, was very similar to that in the crystal.