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General Stereoselective Synthesis of Chemically Differentiated α-Diamino Acids: Synthesis of 2,6-Diaminopimelic and 2,7-Diaminosuberic Acids

✍ Scribed by Hernández, Nicolás; Martín, Víctor S.

Book ID
126446242
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
85 KB
Volume
66
Category
Article
ISSN
0022-3263

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A concise, stereoselective synthesis of
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✍ Philip N Collier; Ian Patel; Richard J.K Taylor 📂 Article 📅 2001 🏛 Elsevier Science 🌐 French ⚖ 63 KB

The preparation of meso-2,6-diaminopimelic acid 1 is described. The key step in the synthesis is Suzuki coupling of the novel organoboron homoalanine equivalent 3 with methyl (2Z)-3-bromo-2-[(tert-butoxycarbonyl)amino]-2-propenoate 5.