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General method for determining the optical purity of phosphines

โœ Scribed by Casey, Jeremiah P.; Lewis, Robert Albert; Mislow, Kurt


Book ID
125940567
Publisher
American Chemical Society
Year
1969
Tongue
English
Weight
266 KB
Volume
91
Category
Article
ISSN
0002-7863

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## Abstract A novel and very accurate method was established for the determination of the optical purity of a peptide by use of the following procedure: (1) hydrolysis of the peptide in deuterium chloride, (2) gas chromatographic separation of each amino acid enantiomer on a chiral phase, and (3) d