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Gas chromatography of amino acids as n-thiocarbonyl ester derivatives

✍ Scribed by B. Halpern; Virginia A. Close; Annemarie Wegmann; J.W. Westley

Publisher
Elsevier Science
Year
1968
Tongue
French
Weight
184 KB
Volume
9
Category
Article
ISSN
0040-4039

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✦ Synopsis

Protein hydrolysates are now routinely analysed by ion exchange chromatography (1) but a complete determination takes at least 3 hours. In addition, the automated amino acid analyzers now used are expensive and have limited application to other problems. Gas chromatography (g.1.c.) offers potential advantages in both speed and sensitivity at a greatly reduced instrumentation cost. However, despite many attempts (2), no entirely satisfactory g.1.c. procedure has been developed.

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