Gas chromatography-mass spectrometry of fatty aldehydes and their oxime derivatives
โ Scribed by G. Phillipou; A. Poulos
- Publisher
- Elsevier Science
- Year
- 1978
- Tongue
- English
- Weight
- 194 KB
- Volume
- 22
- Category
- Article
- ISSN
- 0009-3084
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๐ SIMILAR VOLUMES
A method for analysis of aliphatic aldehydes in biological samples is described. Cyclohexanone is added as internal standard and the samples are treated with hydroxylamine and perchloric acid. The oximes are extracted and converted to the oxime-tert-butyldimethylsilyl derivatives, which are quantita
## Abstract Thermospray (TSP) mass spectrometry has proved to be a useful technique for analysing various highly polar compounds. The use of a quadrupole mass spectrometer equipped with a thermospray/plasmaspray interface in the analysis of more than 30 monosaccharides and sugar derivatives is desc