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Gas chromatographic resolution of enantiomeric and diastereoisomeric amino acid esters on Chirasil-Val capillary column

✍ Scribed by De-Ming Liu

Book ID
112732204
Publisher
Springer
Year
1988
Tongue
English
Weight
227 KB
Volume
25
Category
Article
ISSN
0009-5893

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GC resolution of various D, L-amino acid
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✍ Abe, I. ;Izumi, K. ;Kuramoto, S. ;Musha, S. πŸ“‚ Article πŸ“… 1981 πŸ› John Wiley and Sons 🌐 English βš– 250 KB

## Abstract An enantiomeric mixture of amino acids is derivatized to give the respective __N(O)__‐perfluoroacyl alkyl esters which can be resolved directly by gas chromatography on a Chirasil‐Val capillary column. The retention times, resolution numbers, and elution order are reported.

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✍ Grant Gill Smith; David M. Wonnacott πŸ“‚ Article πŸ“… 1980 πŸ› Elsevier Science 🌐 English βš– 540 KB

An improved method is described for the resolution of enantiomeric isopropyl esters of N-trifluoroacetyl-u-amino acids of nonbasic amino acids using N-docosanoyl-L-valyl-rbutylamide and N-octadecanoyl-L-valyl-t.-valine cyclohexyl ester as mixed chiral phases on 150-ft stainless-steel capillary colum