Gas chromatographic determination of the lower aliphatic primary amines as their Schiff bases
β Scribed by Yasuyuki Hoshika
- Publisher
- Elsevier Science
- Year
- 1975
- Tongue
- English
- Weight
- 385 KB
- Volume
- 115
- Category
- Article
- ISSN
- 1873-3778
No coin nor oath required. For personal study only.
β¦ Synopsis
The identifratlon and qgzntirztive determination Of the lower aIipk.ftic and relatedamines<e.g. i~_foOd,tobaccoandtobaccosmo!;e,dnr_es,natrrralproducts,and bloiogical systems) is a commonIy enconntercd pfobkm in organic analysis. 'The gzs ChiO~~tO~Z?~~C(GC) determination ofthese&nesatfoir,r cO~#~tr~tiOllSiSlimited by adsorption and decomposition in the cofwrm, ghosting phenomena, badly tailed ebtion p&s, and the low sensitivity ofthe compounds in the gas cbromato~aphic detector.
Acomaonmethod
π SIMILAR VOLUMES
The copper(H), mckel(II) and palladmm(I1) complexes of the tetradentate hgands N,N '-1,2-propylenebd5,5-dl-methyl4oxohexan-2-mnne) and N,N'-1,2-propylenebls(6-methyl-4-oxoheptan-2-umne) (H,IVA,pn) were prepared and separated by gas chromatography and reversed-phase liquid chromatography (LC) The lat
A method is described for the determination of residues of those substituted urea and carbamate herbicides which hydrolyze to give an aromatic amine. The 2,4clinitrophenyl derivatives of the amines, .which are amenable to gas chromatography and possess strong electron-captaring properties, are prepa