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Gas chromatographic determination of serum branched-chain α-keto acids derivatized by extractive alkylation

✍ Scribed by I. Penttilä; A. Huhtikangas; J. Herranen; O. Moilanen


Publisher
Elsevier Science
Year
1985
Weight
443 KB
Volume
338
Category
Article
ISSN
0378-4347

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The α-keto acids of branched-chain amino
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By use of a relatively new mixed stationary phase, complete separation of the branchedchain cy-keto acids as O-trimethylsilyl-quinoxalinol derivatives is achieved within 10 min by packed column gas chromatography. Precise quantification of less than 5 nmol of cr-keto acids in biological samples is p