𝔖 Bobbio Scriptorium
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From Triple-Decker to Metallabenzene: A New Generation of Sandwich Complexes

✍ Scribed by Dipl.-Chem. Ulrike Bertling; Dr. Ulli Englert; Prof. Dr. Albrecht Salzer

Publisher
John Wiley and Sons
Year
1994
Tongue
English
Weight
257 KB
Volume
33
Category
Article
ISSN
0044-8249

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✦ Synopsis

V=6213(7)AZ. Z = 4. , I ~, , , ~~ = l.l6X A total of 12975 unique data points Nere collected (Mo,,. i = 0.71049 A, p =1.60cm-'. 20<50-) of which 4386 had F>4u(k')

and werc used for structure retinement Thete data bets were collected by using a Rigaku AFC-5R diffractometer at 296 K. An absorption correction. using the pi-ogram DIF.4BS. wits applied which resulted in transmtssion factors ranging from 0.88 to 1.12. The structure was solved by direct methods and refined by full-mati I& least-squares method (TEXSAN. Molecular Structure Corp.. USA) h i t h aniwtropic thermal parameters for non-hydrogen atoms, except for five carbon i i t o n i b of the hutyl groups. Because of the disorder of the hutbl group.

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