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Friedel–Crafts hydroxyalkylation: reaction of anisole with paraformaldehyde catalyzed by zeolites in supercritical CO2

✍ Scribed by Mercedes Álvaro; Debasish Das; Monica Cano; Hermenegildo Garcia

Book ID
114046302
Publisher
Elsevier Science
Year
2003
Tongue
English
Weight
165 KB
Volume
219
Category
Article
ISSN
0021-9517

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✍ Norio Sakai; Toshihiro Hamajima; Takeo Konakahara 📂 Article 📅 2002 🏛 Elsevier Science 🌐 French ⚖ 84 KB

A catalytic amount of copper(II) trifluoromethanesulfonate (Cu(OTf) 2 ) in the presence of trimethylchlorosilane (TMSCl) effectively promoted the aminomethylation of indoles bearing a variety of functional groups with a N-silyl-N,O-acetal in good to excellent yields.