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Formation of methyl ester of salicyluric acid during quantitation of salicyluric acid in urine by high-pressure liquid chromatography

โœ Scribed by R. O. Day; S. H. Dromgoole; D. E. Furst; C. Hignite; H. E. Paulus

Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
384 KB
Volume
70
Category
Article
ISSN
0022-3549

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Bile acids have been separated by high-pressure liquid chromatography. The free acids were derivatized to their phenacyl esters by treatment with triethylamine and a-bromoacetophenone. The stationary phase was a C,,, Partisil ODS column. A dual-solvent, stepwise gradient system was used for the mobi