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FORMATION OF FORMALDEHYDE FROM GLYCEROL-C 14 BY PROPIONIBACTERIUM 1

✍ Scribed by Leaver, F. W.

Book ID
126974482
Publisher
American Chemical Society
Year
1951
Tongue
English
Weight
282 KB
Volume
73
Category
Article
ISSN
0002-7863

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## Abstract [1‐^14^C]‐2,2‐Difluoroethene was synthesized from [^14^C]‐formaldehyde using a modification of the Wadsworth‐Emmons reaction, __via__ formation of the intermediate (EtO)~2~P(O)CF~2~^14^CH~2~OSiMe~3~. This highly volatile product was collected in a liquid nitrogen trap at a purity of >97