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Formation of an iridium σ-cyclopropane complex by the intramolecular activation of a cyclopropylphosphine: Rearrangement to a chelating σ-vinyl complex

✍ Scribed by Wiley J. Youngs; Barbara L. Simms; James A. Ibers

Publisher: Elsevier Science
Year: 1984
Tongue: English
Weight: 888 KB
Volume: 272
Category: Article
ISSN: 0022-328X
DOI: 10.1016/0022-328x(84)80472-6

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The residue was extracted with Et,O (50 nil) to give a suspension of the red solid product in Et,O. The product was then filtered off and dried in vacuo (31 Yo). Recrystallization of the powder from Et,O:pyridine (90.10) yielded red crystals suitable for X-ray diffraction. Elemental analysis calcd f