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Formation of a tricyclic phosphorane in the reaction of diethylamino-(2-acetylphenyl)-phenylphosphonite with acetic acid

✍ Scribed by F. S. Mukhametov; É. E. Korshin

Book ID
112443718
Publisher
Springer
Year
1985
Tongue
English
Weight
68 KB
Volume
34
Category
Article
ISSN
1573-9171

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## Abstract Reduction of the isoprene—PCl~3~ adduct 1 with magnesium powder, or with Si~2~Cl~6~, furnished __P__‐chloro‐3‐methyl‐phosphol‐2‐ene, 2, in satisfactory yield. Further reduction of 2 with Si~2~Cl~6~ gave the new trichlorosilyl‐3‐methylphosphol‐2‐ene, 3. The reaction of 2 with magnesium p