Formation and Properties of Ascorbigen
β Scribed by G. Kiss
- Publisher
- John Wiley and Sons
- Year
- 1966
- Tongue
- English
- Weight
- 115 KB
- Volume
- 5
- Category
- Article
- ISSN
- 0044-8249
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## Abstract Polycarbazole (PCz) was synthesized by chemical polymerization of carbazole in acetonitrile medium using ammonium persulfate as oxidant. The selection of solvent, concentration of the monomer, composition of the solvent, polymerization time, temperature, and pH were optimized to obtain
17a-(2-Dimethylaminoethyl)-17a-aza-D-homo-5androsten -3/3 -01 (XIVbMethod D-Compound X (2.0 9.) was dissolved in 30 ml. of dioxane, a solution of 1.0 g. of lithium aluminum hydride in 300 ml. of dioxane was added, and the mixture was refluxed for 48 hr. Excess hydride was destroyed with water. The i