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Fluorometric reagents for primary amines. Syntheses of 2-alkoxy- and 2-acyloxy-3(2H)-furanones

✍ Scribed by Weigele, Manfred.; Tengi, John P.; De Bernardo, Silvano.; Czajkowski, Ronald.; Leimgruber, Willy.

Book ID: 121504929
Publisher: American Chemical Society
Year: 1976
Tongue: English
Weight: 279 KB
Volume: 41
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00864a051

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## Abstract The 6‐hydroxy‐2H‐pyran‐3(6H)‐ones 1a–d are esterified stereoselectively with acetic and formic acid, and with several amino acids and peptide derivatives using the DCC/DMAP method. The direct synthesis of the 6‐alkoxy derivatives 3g–k is also studied.