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Fluoroalkyl-s-triazines

✍ Scribed by Thomas S. Croft; Carl F. Snyder Jr.

Book ID: 112123064
Publisher: Journal of Heterocyclic Chemistry
Year: 1973
Tongue: English
Weight: 240 KB
Volume: 10
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.5570100610

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The a-aminoheterocycle (0.1 mol) is dissolved in anhydrous benzene or toluene and dropped into a boiling mixture of oxalyl chloride (0.4-0.5 mol) and anhydrous benzene or toluene (1-2 mol). The whole is boiled under reflux until evolution of gas is completed ( 2 4 h). After filtration (crystalline p